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Ders Tanımı

Ders Kodu Yarıyıl T+U Saat Kredi AKTS
INSTRUMENTAL ANALYSIS LABORATORY KIM 308 6 0 + 4 4 6
Ön Koşul Dersleri Instrumental analysis course must be taken before
Önerilen Seçmeli Dersler
Dersin Dili Türkçe
Dersin Seviyesi Lisans
Dersin Türü ZORUNLU
Dersin Koordinatörü Prof.Dr. MUSTAFA GÜLFEN
Dersi Verenler
Dersin Yardımcıları Research assistants
Dersin Kategorisi Alanına Uygun Temel Öğretim
Dersin Amacı
For students studying in Chemistry department, application of theoretical knowledge by using laboratory apparatus in order to obtain quantitative and qualitative information about the composition and structure of a Matter
For this purpose, learning how to analyse various samples and obtain teoretical information about instruments
Learning how to solve the instrumental problems if it occurs using different instrumental approaches,
In conclusion, preparing students for marketing conditions and requirements
Dersin İçeriği
Introduction to Laboratory Analysis, Laboratory Regulations, Risk Assessment, Qualitative and Quantitative Analysis Techniques, Calibration, UV-Vis. spectrometry, Atomic absorption spectrometry and other similar techniques, Plasma spectrometries. Infrared spectrometry, Assessment of IR Spectrums, Assessment of NMR spectrums, Mass spectrometry and assessment of its spectrums, Chromatographic methods and evaluating spectrums.
Dersin Öğrenme Çıktıları Öğretim Yöntemleri Ölçme Yöntemleri
1 - 1 - 2 - 4 - 13 - A - C -
2 - do analysis by using instrumental analysis techniques 1 - 2 - 6 - 13 - B - C -
3 - solve the instrumental problems and own the ability and experience to bring solutions for the problems 1 - 2 - 6 - 13 - B - C -
4 - interpret the analysis results 1 - 2 - 6 - 13 - B - C -
5 - develop proper method for the analysis of certain group of compounds 1 - 2 - 6 - 13 - B - C -
6 - select proper method when they encounter an unknown sample 1 - 2 - 6 - 13 - B - C -
7 - select a proper method for the analysis of mixtures 1 - 2 - 6 - 13 - B - C -
8 - use different methods simultaneously for the analysis 1 - 2 - 6 - 13 - A - C -
Öğretim Yöntemleri: 1:Lecture 2:Question-Answer 6:Motivations to Show 13:Lab / Workshop 4:Drilland Practice
Ölçme Yöntemleri: B:Oral Exam C:Homework A:Testing

Ders Akışı

Hafta Konular ÖnHazırlık
1 Introduction, Laboratory regulations, Risk assessment, Preparing Experiment groups [1] Page ii-vi
2 Principal knowledge, Calibration techniques used in theoretical analysis [1] Page 1-6
3 Determination of iron in canned drinks by AAS [1] Page 8-10
4 Determination of fatty acid content in various fats by GC [1] Page 11-16
5 Determination of Sodium and Potassium by using Flame Emission Spectrometry [1] Page 17-19
6 ICP-Atomic emission spectrometry [1] Page 20-24
7 Determination of aspirin and caffein in pain killers by UV spectrometry [1] Page 25-27
8 Quantitative analysis by using IR spectrometry [1] Page 28-44
9 MID-TERM EXAM
10 Ion Exchange chromatography [1] Page 45-47
11 Molecular mass spectrometry [1] Page 48-56
12 NMR Spectrometry [1] Page 57-65
13 Recovery week
14 Recovery week

Kaynaklar

Ders Notu [1]. Prof.Dr. Mustafa Şahin DÜNDAR, Instrumental Analysis Lab. Book, Sakarya, 2008.
Ders Kaynakları [2]. Principles of Instrumental Analysis, Skoog-Holler-Nieman: Esma Kılıç, Fitnat Köseoğlu, Hamza Yılmaz (Translation Editors), Bilim yayıncılık, Ankara, 2000.

Döküman Paylaşımı


Dersin Program Çıktılarına Katkısı

No Program Öğrenme Çıktıları KatkıDüzeyi
1 2 3 4 5
1 Informs the experienced and non experienced listener groups about the subjects related to chemistry and clearly transfers the ideas, problems and solution techniques written and orally. X
2 Shows the capability of doing advance level scientific studies independently by critical thought and learning to learn. X
3 Produces the solutions by taking the responsibilities in the case of complex situations which is unpredictable in advance in chemistry area applications.
4 Plans activities and directs them to improve the ability of his or her workers in industry in the field of chemistry. X
5 Has enough foreign language knowledge to be able to follow the new technologies related to her/his area and to be able to communicate with her/his colleagues. X
6 In addition to having knowledge at satisfactory level about computer hardware, software, data processing, uses information and communication technologies which is necessary for her/his area. X
7 Protects the social ethical values at the stage of collection, evaluation and publishing of data related to chemistry area.
8 Has enough knowledge and consciousness about job security, health of workers, social security rights, quality control and management and environmental protection. X
9 Understands the industrial process and solves the problems faced in chemistry area. X
10 X
11 X

Değerlendirme Sistemi

YARIYIL İÇİ ÇALIŞMALARI SIRA KATKI YÜZDESİ
AraSinav 1 30
KisaSinav 1 10
KisaSinav 2 10
Odev 1 10
PerformanGoreviLabaratuvar 1 40
Toplam 100
Yıliçinin Başarıya Oranı 60
Finalin Başarıya Oranı 40
Toplam 100

AKTS - İş Yükü

Etkinlik Sayısı Süresi(Saat) Toplam İş yükü(Saat)
Course Duration (Including the exam week: 16x Total course hours) 16 4 64
Hours for off-the-classroom study (Pre-study, practice) 16 2 32
Mid-terms 1 10 10
Quiz 2 5 10
Assignment 1 5 5
Performance Task (Laboratory) 1 20 20
Final examination 1 10 10
Toplam İş Yükü 151
Toplam İş Yükü /25(s) 6.04
Dersin AKTS Kredisi 6.04
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